方解石热释光定年技术的发展历史与展望

doi:10.3969/j.issn.0253-4967.2024.03.011

地震地质 ›› 2024, Vol. 46 ›› Issue (3): 699-722.DOI: 10.3969/j.issn.0253-4967.2024.03.011

方解石热释光定年技术的发展历史与展望

秦可心¹⁾(), 胡贵明¹⁾^,^*(), 刘静¹^,²⁾, 沈续文¹⁾, 高云鹏¹⁾, 王文鑫¹⁾, 温欣语¹⁾, 蒋帅宇¹⁾

¹⁾ 天津大学, 地球系统科学学院, 表层地球系统科学研究院, 天津 300072
²⁾ 中国地震局地质研究所, 地震动力学国家重点实验室, 北京 100029

收稿日期:2023-05-18 修回日期:2023-09-18 出版日期:2024-06-20 发布日期:2024-07-19
通讯作者: *胡贵明, 男, 1989年生, 博士, 助理研究员, 主要从事释光方面的研究, E-mail: guiming_32@tju.edu.cn。
作者简介:
秦可心, 女, 1999年生, 现为天津大学地球系统科学学院地理学专业在读硕士研究生, 主要从事释光低温热年代学和构造地貌方面的研究, E-mail: qin_kexin@outlook.com。
基金资助:
国家自然科学基金(42030305); 国家自然科学基金(42202212); 中国博士后国际交流计划引进项目(YJ20210146); 中国博士后科学基金项目(2021M702425); 天津市自然科学基金青年项目(23JCQNJC02000)

DEVELOPMENT AND PROSPECT OF THERMOLUMINESCENCE DATING BY USING CALCITE

QIN Ke-xin¹⁾(), HU Gui-ming¹⁾^,^*(), LIU-ZENG Jing¹^,²⁾, SHEN Xu-wen¹⁾, GAO Yun-peng¹⁾, WANG Wen-xin¹⁾, WEN Xin-yu¹⁾, JIANG Shuai-yu¹⁾

¹⁾ Institute of Surface-Earth System Science, School of Earth System Science, Tianjin University, Tianjin 300072, China
²⁾ State Key Laboratory of Earthquake Dynamics, Institute of Geology, China Earthquake Administration, Beijing 100029, China

Received:2023-05-18 Revised:2023-09-18 Online:2024-06-20 Published:2024-07-19

摘要/Abstract

摘要：

矿物晶体中累积的释光信号与其暴露在辐射环境中的时间相关, 可用于测定沉积物年代。近年来, 依托石英和长石2种矿物释光信号的测年方法日臻成熟, 但这2种矿物的释光信号过早饱和, 限制了其测年上限(通常<300ka)。前人研究表明, 方解石亦有可能成为热释光测年材料, 因为其热释光信号对剂量响应的灵敏度高, 且特征饱和剂量约可达3 000~5 000Gy, 有望将释光测年范围扩展至第四纪尺度。特别地, 这一技术的发展也将拓展目前仅限于剥露速率极高地区的释光低温热年代学的应用范围, 使其更好地贡献于地貌演化和构造活动的研究。文中对方解石热释光的基本原理和测年流程进行了简要概括, 总结了方解石热释光测年应用及动力学参数的研究成果。此外, 利用方解石热释光技术对虎跳峡段的基岩样品进行了测试, 结果表明, ITL-235℃释光信号可用于该地区剥露历史的恢复工作。同时, 文中基于上述内容讨论了方解石热释光技术的应用潜力和待解决问题, 以期为该技术在构造地貌领域的应用提供帮助。

关键词: 方解石, 热释光, 低温热年代学, 虎跳峡

Abstract:

The accumulation of luminescence signals in mineral crystals correlates with the duration of exposure to radiation. This phenomenon has been utilized as a tool for measuring sediment age and has found extensive application in various research endeavors. While quartz and feldspar luminescence signals have been utilized for dating in recent years, their effectiveness is constrained by early saturation, limiting their dating range to less than 300ka. In contrast, calcite exhibits high sensitivity to dose responses of thermoluminescence signals and possesses a characteristic saturation dose that can reach levels of 3 000-5 000Gy, making it a promising material for thermoluminescence dating. This has the potential to extend the age range of luminescence dating to the Quaternary period and broaden the application scope of low-temperature thermochronology. Providing quantitative descriptions of bedrock exhumation history through low-temperature thermochronology can offer crucial data support for understanding the interconnected relationship between tectonic activity, climate influences, and geomorphic evolution. Low-temperature thermoluminescence thermochronology, characterized by its high resolution and low closure temperature, presents advantages over commonly used apatite U-Th/He thermochronology in elucidating the excavation history of the Earth’s crust surface(approximately 1~2km). However, traditional minerals utilized for reconstructing bedrock cooling history, such as quartz and feldspar, exhibit rapid saturation, limiting the study period to less than 200ka. In contrast, calcite boasts an exceptionally high characteristic saturation dose and lower dose rate, making it a promising new dating mineral that extends the upper limit of low-temperature thermoluminescence thermochronology beyond 0.5Ma.

This paper begins by introducing the principle and application of thermoluminescence dating, followed by an overview of commonly used techniques for measuring dose rate and equivalent dose. The thermoluminescence dating process primarily involves equivalent dose measurement and dose rate measurement. Considerable research has been conducted on equivalent dose, and newly developed methods such as single aliquot regenerative dose, multiple aliquot regenerative dose, and multiple aliquot-additive dose have addressed issues related to sensitivity changes caused by heating, thereby enhancing the accuracy of dating results. Additionally, the paper summarizes recent advancements in calcite thermoluminescence dating and kinetic parameters. To validate the method, we performed thermoluminescence dating analysis on calcite grains in bedrock samples collected from the Tiger Leap Gorge of the Jinsha river.

After passing through Shigu, the Jinsha river experiences a sudden change in flow direction, carving its way through the Yulong-Haba mountain range to create the renowned “Tiger Leaping Gorge.” This geographic feature is characterized by active tectonics and intense river erosion, making it an ideal site for investigating the interplay among tectonics, climate, and surface processes. However, the Tiger Leaping Gorge primarily comprises limestone and griotte, lacking minerals such as apatite and zircon necessary for traditional low-temperature thermochronology dating(only exposed in the Upper Tiger Leaping Gorge). Consequently, it presents an ideal setting for exploring calcite low-temperature thermoluminescence thermochronology. SAR-ITL can detect the 280℃ thermoluminescence peak signal of calcite at 235℃, effectively mitigating the influence of spurious thermoluminescence. Moreover, the number of calcite grains required is lower than that of the MAAD test. The findings highlight the potential of this method for estimating the exhumation rate of carbonate rock. To facilitate its more effective utilization in the field of tectonic geomorphology, we address the challenges and potential applications of calcite thermoluminescence dating.

Key words: Calcite, Thermoluminescence, Low-temperature thermochronology, Tiger Leaping Gorge

秦可心, 胡贵明, 刘静, 沈续文, 高云鹏, 王文鑫, 温欣语, 蒋帅宇. 方解石热释光定年技术的发展历史与展望[J]. 地震地质, 2024, 46(3): 699-722.

QIN Ke-xin, HU Gui-ming, LIU-ZENG Jing, SHEN Xu-wen, GAO Yun-peng, WANG Wen-xin, WEN Xin-yu, JIANG Shuai-yu. DEVELOPMENT AND PROSPECT OF THERMOLUMINESCENCE DATING BY USING CALCITE[J]. SEISMOLOGY AND GEOLOGY, 2024, 46(3): 699-722.

图/表 14

图1 方解石、钾长石、石英释光测年范围对比(修改自Duller et al., 2018)

Fig. 1 Luminescence dating ranges of calcite, potassium feldspar and quartz(modified from Duller et al., 2018).

图2 电子捕获和释放的示意图(修改自King et al., 2016a). a 矿物晶格缺陷示意图, 如空穴、间隙、杂质; b 自由电子受到辐照后被陷阱捕获; c 当样品受到热激发时, 被捕获的电子由于温度升高逃离捕获点并重新与发光中心结合, 以光的形式释放一部分能量

Fig. 2 Schematic diagrams of electron trap and release( modified from King et al., 2016a).

图3 附加剂量法与再生剂量法(修改自Aitken, 1985) a P为古剂量, I为校正部分, Q为获得的等效剂量, N为自然剂量, β为实验室添加剂量, 至少需要构建2个附加剂量点, 图中的N+β、 N+2β; b N为自然剂量, 通过内插至热释光信号-剂量响应曲线获得

Fig. 3 Additive dose method and regenerative dose method(modified from Aitken, 1985).

图4 MAR法在330℃获得的热释光信号-剂量响应曲线

Fig. 4 Dose response curve of the MAR-TL at 330℃.

图5 MAAD法在330℃获得的热释光信号-剂量响应曲线

Fig. 5 Dose response curve of the MAAD-TL at 330℃.

图6 坪区实验(修改自Aitken, 1985) N为某测片组自然热释光曲线, N+β是剩余测片组经实验室附加剂量辐照后的自然+人工热释光曲线; 虚线表示2条热释光曲线的比值在0.47附近出现坪区

Fig. 6 Plateau-Test(modified from Aitken, 1985).

图7 高饱和水平样品坪区实验(修改自Bassinet et al., 2006) TLn为自然发光曲线, R1—R4为给定不同附加剂量后的发光曲线。圆点为等效剂量值, 在峰值附近(±20℃)存在坪区

Fig. 7 Plateau-Test of high equivalent dose sample(modified from Bassinet et al., 2006).

图8 衰减校正示意图(修改自King et al., 2016b) a、 b分别为50℃、 225℃红外激发释光信号的异常衰减校正, t*为辐照时间的一半与延迟测量时间之和

Fig. 8 Fading correction(modified from King et al., 2006b).

表1 方解石热释光应用统计

Table1 Statistical summary of calcite thermoluminescence studies

文献	测年样品类型	测年结果/ka
Johnson, 1966	接触变质	岩浆温度
Johnson et al., 1967	贝壳方解石	3.16±0.16、6.00、2.10±0.3、6.10±0.8、7.25±0.2、8.70±0.2、9.75±0.25、7.00×10¹、7.00×10³、1.80×10⁴、3.30×10⁴、5.00×10⁴、1.00×10⁵
Debenham et al., 1984	石笋方解石	3.00×10²
Matsuoka et al., 1983	鱼骨化石	测量了s和E
Debenham et al., 1984	石笋方解石	26±13、181±49、131±27、205±36、160±20、168±27、178±32、110±20、107±18、103±17、103±14、157±19、86±30、187±41、163±64、241±47、279±46、262±39、233±69、169±34、167±57、128±18、159±22、281±33、229±21、259±31、298±33
Franklin et al., 1988	次生方解石脉	5500、4100
Ninagawa et al., 1992	扇贝科方解石壳	440±60、(680±120)ka、(640±110)ka、(530±90)ka、540±100、550±140、690±180、560±130、480±110、480±140、360±100、550±90、670±110、500±70、490±60、550±70、410±50、380±50、370±50、290±40、100±20、130±20、110±20、120±30
Carmichael et al., 1994	贝壳方解石	存在信号损失
Ninagawa et al., 1994	贝壳方解石	400±60、400±40、150±20、17±2、12±2
Lirizis et al., 1994	建筑石灰石	3.7±0.45、1.7±0.45
Engin et al., 1997	钙华	828±93
Roque et al., 2001	洞穴碎石	18.1±2.6、20.2±2.0
Ninagawa et al., 2001	石灰岩样品	(280~322)±16、(722~877)±99、(193~208)±10、(241~259)±11、(166~174)±12、(158~163)±9、(950~1060)±127
Misdaq et al., 2002	石笋和钟乳石	121.06±10、116.00±7、110.00±6、104.00±6、81.00±7、69.00±4
Polikreti et al., 2003	大理石器物	2.57±0.441
Liritzis, 2010	岩板中的方解石	3.52±0.54
Guibert et al., 2015	墙上的石灰石	36.9±2.3
	洞穴入口碎石	34.3±2.9
Yee et al., 2018	钟乳石	805.4±7.6、789.8±7.8、708.9±7.9、761.6±8.1、707.3±8.3

表1 方解石热释光应用统计

Table1 Statistical summary of calcite thermoluminescence studies

文献	测年样品类型	测年结果/ka
Johnson, 1966	接触变质	岩浆温度
Johnson et al., 1967	贝壳方解石	3.16±0.16、6.00、2.10±0.3、6.10±0.8、7.25±0.2、8.70±0.2、9.75±0.25、7.00×10¹、7.00×10³、1.80×10⁴、3.30×10⁴、5.00×10⁴、1.00×10⁵
Debenham et al., 1984	石笋方解石	3.00×10²
Matsuoka et al., 1983	鱼骨化石	测量了s和E
Debenham et al., 1984	石笋方解石	26±13、181±49、131±27、205±36、160±20、168±27、178±32、110±20、107±18、103±17、103±14、157±19、86±30、187±41、163±64、241±47、279±46、262±39、233±69、169±34、167±57、128±18、159±22、281±33、229±21、259±31、298±33
Franklin et al., 1988	次生方解石脉	5500、4100
Ninagawa et al., 1992	扇贝科方解石壳	440±60、(680±120)ka、(640±110)ka、(530±90)ka、540±100、550±140、690±180、560±130、480±110、480±140、360±100、550±90、670±110、500±70、490±60、550±70、410±50、380±50、370±50、290±40、100±20、130±20、110±20、120±30
Carmichael et al., 1994	贝壳方解石	存在信号损失
Ninagawa et al., 1994	贝壳方解石	400±60、400±40、150±20、17±2、12±2
Lirizis et al., 1994	建筑石灰石	3.7±0.45、1.7±0.45
Engin et al., 1997	钙华	828±93
Roque et al., 2001	洞穴碎石	18.1±2.6、20.2±2.0
Ninagawa et al., 2001	石灰岩样品	(280~322)±16、(722~877)±99、(193~208)±10、(241~259)±11、(166~174)±12、(158~163)±9、(950~1060)±127
Misdaq et al., 2002	石笋和钟乳石	121.06±10、116.00±7、110.00±6、104.00±6、81.00±7、69.00±4
Polikreti et al., 2003	大理石器物	2.57±0.441
Liritzis, 2010	岩板中的方解石	3.52±0.54
Guibert et al., 2015	墙上的石灰石	36.9±2.3
	洞穴入口碎石	34.3±2.9
Yee et al., 2018	钟乳石	805.4±7.6、789.8±7.8、708.9±7.9、761.6±8.1、707.3±8.3

图 9 方解石动力学参数频率因子s、陷阱深度E、捕获电子寿命τ的分布

Fig. 9 The distribution of calcite frequency factor, trap depth and thermochronometric age.

图 10 虎跳峡河段采样点

Fig. 10 Map showing sampling locations.

表2 MAAD测量程序

Table2 Thermoluminescence measurement sequence of MAAD

步骤	程序	结果
1	附加剂量, D_i
2	预热(T=240℃, 0s)	去除不稳定信号
3	TL(5℃/s)	热释光信号强度, L_n/L_x
4	称重	质量归一化

图 11 a—c 利用MAAD-TL测量HT21获得的热释光信号-剂量响应曲线; d 利用MAAD-TL测量获得HT21的等效剂量; e 利用SAR-ITL测量获得HT23-13的等效剂量黑色方形点为每组测片的平均值, 黑色实线为单一饱和指数函数 y = y 0 + a × 1 - e x p ~ - D e D 0拟合结果

Fig. 11 Dose response curves of the MAAD-TL at 255℃, 285℃, 330℃(a—c); De values from the MAAD-TL for HT21(d); De values from the SAR-ITL for HT23-13(e).

表3 SAR-ITL测量程序

Table3 Thermoluminescence measurement sequence of SAR-ITL

步骤	程序	结果
1	再生剂量, D_i
2	预热(T=230℃, 0s)	去除不稳定信号
3	ITL-100s(220~260℃,间隔5℃, 5℃/s)	获得等温衰退曲线, L_n/L_x
4	检验剂量, D_t=120Gy	灵敏度校正
5	预热(T=230℃, 0s)	去除不稳定信号
6	ITL-100s(220~260℃,间隔5℃, 5℃/s)	获得等温衰退曲线, T_n/T_x
7	加热(T=300℃, 10s)	清除累积信号
8	循环上述步骤

参考文献 127

[1]	刘静, 张金玉, 葛玉魁, 等. 2018. 构造地貌学: 构造-气候-地表过程相互作用的交叉研究[J]. 科学通报, 63(30): 3070—3088.
	LIU Jing, ZHANG Jin-yu, GE Yu-kui, et al. 2018. Tectonic geomorphology: An interdisciplinary study of the interaction among tectonic climatic and surface processes[J]. Science Bulletin, 63(30): 3070—3088 (in Chinese).
[2]	刘静, 曾令森, 丁林, 等. 2009. 青藏高原东南缘构造地貌, 活动构造和下地壳流动假说[J]. 地质科学, 44(4): 1227—1255.
	LIU Jing, ZENG Ling-sen, DING Lin, et al. 2009. Tectonic geomorphology, active tectonics and lower crustal channel flow hypothesis of southeastern Tibetan plateau[J]. Chinese Journal of Geology, 44(4): 1227—1255 (in Chinese).
[3]	濮逸铖, 覃金堂, 陈杰, 等. 2022. 基于Sobol'方法的释光热年代模型参数敏感性分析[J]. 第四纪研究, 42(5): 1430—1442.
	PU Yi-cheng, QIN Jin-tang, CHEN Jie, et al. 2022. Sobol’ sensitivity analysis of luminescence thermochronology model[J]. Quaternary Sciences, 42(5): 1430—1442 (in Chinese).
[4]	覃金堂, 陈杰, 李涛. 2020. 阿尔金断裂带中段现代沉积物样品钾长石红外激发后红外释光的残留信号: 对年轻古地震事件测年的指示意义[J]. 地震地质, 42(4): 981—992. doi: 10.3969/j.issn.0253-4967.2020.04.014.
	QIN Jin-tang, CHEN Jie, LI Tao. 2020. Residual post-IR IRSL signals of potassium feldspar from modern sag pond deposits of Central Altyn Tagh Fault: Implication for dating young paleoseismic events[J]. Seismology and Geology, 42(4): 981—992 (in Chinese).
[5]	石许华, 王二七, 王刚, 等. 2008. 青藏高原东南缘玉龙雪山(5 596m)晚新生代隆升的侵蚀与构造控制作用[J]. 第四纪研究, 28(2): 222—231.
	SHI Xu-hua, WANG Er-qi, WANG Gang, et al. 2008. Late Cenozoic uplift of the Yulong Snow Mountain(5 596m), SE Tibetan Plateau, caused by erosion and tectonic forcing[J]. Quaternary Sciences, 28(2): 222—231.
[6]	王同利. 2006. 释光测年中几种年剂量测量方法的对比[D]. 北京: 中国地震局地质研究所.
	WANG Tong-li. 2006. A comparison of methods for the annual radiation dose determination in luminescence dating[D]. Institute of Geology, China Earthquake Administration, Beijing (in Chinese).
[7]	王维达. 2009. 古陶瓷热释光测定年代的研究和进展[J]. 中国科学(E辑), 39(11): 1767—1799.
	WANG Wei-da. 2009. Study and progress of the thermoluminescence dating of the ancient pottery and porcelain[J]. Science in China(Ser E), 39(11): 1767—1799 (in Chinese).
[8]	郑勇, 李海兵, 潘家伟, 等. 2022. 长江第一弯虎跳峡的贯通——来自于地表地貌和弹性挠曲的数值模拟分析[J]. 地质学报, 96(8): 2942—2954.
	ZHENG Yong, LI Hai-bing, PAN Jia-wei, et al. 2022. Connection of the Tiger Leaping Gorge near the First Bend of the Yangtze River: New insights from numerical modelling of geomorphology and elastic flexure deformation[J]. Acta Geologica Sinica, 96(8): 2942—2954.
[9]	Aitken M J, Bowman S G E. 1975. Thermoluminescent dating: Assessment of alpha particle contribution[J]. Archaeometry, 17(1): 132—138.
[10]	Atkinson T, Harmon R, Smart P, et al. 1978. Palaeoclimatic and geomorphic implications of ²³⁰Th/²³⁴U dates on speleothems from Britain[J]. Nature, 272(5648): 24—28.
[11]	Aitken M J, Zimmerman D W, Fleming S. 1968. Thermoluminescent dating of ancient pottery[J]. Nature, 219(3): 442—445.
[12]	Aitken M J. 1985. Thermoluminescence Dating[M]. Cambridge University Press, Cambridge.
[13]	Aitken M J. 1998. Introduction to Optical Dating: The Dating of Quaternary Sediments by the Use of Photon-stimulated Luminescence[M]. Clarendon Press, Oxford.
[14]	Bassinet C, Mercier N, Miallier D, et al. 2006. Thermoluminescence of heated quartz grains: Intercomparisons between SAR and multiple-aliquot additive dose techniques[J]. Radiation Measurements, 41(7-8): 803—808.
[15]	Berger G W, Anderson P M. 1994. Thermoluminescence dating of an Arctic lake core from Alaska[J]. Quaternary Science Reviews, 13(5-7): 497—501.
[16]	Blair M W, Yukihara E G, Mckeever S W S. 2005. Experiences with single-aliquot OSL procedures using coarse-grain feldspars[J]. Radiation Measurements, 39(4): 361—374.
[17]	Bouscary C, King G E. 2022. Luminescence thermochronometry of feldspar minerals: Optimisation of measurement conditions for the derivation of thermal kinetic parameters using isothermal holding experiments[J]. Quaternary Geochronology, 67: 1—14.
[18]	Brookfield M E. 1998. The evolution of the great river systems of southern Asia during the Cenozoic India-Asia collision: Rivers draining southwards[J]. Geomorphology, 22(3-4): 285—312.
[19]	Carmichael L A, Sanderson D C W, Riain S N. 1994. Thermoluminescence measurement of calcite shells[J]. Radiation Measurements, 23(2-3): 455—463.
[20]	Chithambo M L, Pagonis V, Ogundare F O. 2014. Spectral and kinetic analysis of thermoluminescence from manganiferous carbonatite[J]. Journal of Luminescence, 145: 180—187.
[21]	Clark M K, Schoenbohm L M, Royden L H, et al. 2004. Surface uplift, tectonics, and erosion of eastern Tibet from large-scale drainage patterns[J]. Tectonics, 23(1): 1—20.
[22]	Clark P A, Templer R H. 1988. Dating thermoluminescence samples which exhibit anomalous fading[J]. International Journal of Radiation Applications and Instrumentation(Part D), Nuclear Tracks and Radiation Measurements, 14(1-2): 139—141.
[23]	Debenham N, Aitken M. 1984. Thermoluminescence dating of stalagmitic calcite[J]. Archaeometry, 26(2): 155—170.
[24]	Du J H, Wang X L. 2014. Optically stimulated luminescence dating of sand-dune formed within the Little Ice Age[J]. Journal of Asian Earth Sciences, 91: 154—162.
[25]	Duller G A T, Penkman K E H, Wintle A G. 2009. Assessing the potential for using biogenic calcites as dosemeters for luminescence dating[J]. Radiation Measurements, 44(5-6): 429—433.
[26]	Duller G A T, Bøtter-Jensen L, Murray A S. 2000. Optical dating of single sand-sized grains of quartz: Sources of variability[J]. Radiation Measurements, 32(5-6): 453—457.
[27]	Duller G A T. 2015. The Analyst software package for luminescence data: Overview and recent improvements[J]. Ancient TL, 33(1): 35—42.
[28]	Duller G A T, Roberts H M. 2018. Seeing snails in a new light[J]. Elements: An International Magazine of Mineralogy, Geochemistry, Petrology, 14(1): 39—43.
[29]	Durrani S A, Khazal K A R, Ali A. 1977. Temperature and duration of the shadow of a recently-arrived lunar boulder[J]. Nature, 266(5601): 411—415.
[30]	Engin B, Güven O. 1997. Thermoluminescence dating of Denizli travertines from the southwestern part of Turkey[J]. Applied Radiation Isotopes, 48(9): 1257—1264.
[31]	Engin B, Güven O. 2000. The effect of heat treatment on the thermoluminescence of naturally-occurring calcites and their use as a gamma-ray dosimeter[J]. Radiation Measurements, 32(3): 253—272.
[32]	Franklin A D, Hornyak W F, Tschirgi A A. 1988. Thermoluminescence dating of Tertiary period calcite[J]. Quaternary Science Reviews, 7(3-4): 361—365.
[33]	Göksu H Y, Pennycook S J, Brown L M. 1988. Thermoluminescence and cathodoluminescence studies of calcite and MgO: Surface defects and heat treatment[J]. International Journal of Radiation Applications and Instrumentation(Part D), Nuclear Tracks and Radiation Measurements, 14(3): 365—368.
[34]	Gong Z, Sun J, Lü T, et al. 2014. Investigating the optically stimulated luminescence dose saturation behavior for quartz grains from dune sands in China[J]. Quaternary Geochronology, 22: 137—143.
[35]	Gourbet L, Leloup P H, Paquette J L, et al. 2017. Reappraisal of the Jianchuan Cenozoic Basin stratigraphy and its implications on the SE Tibetan Plateau evolution[J]. Tectonophysics, 70: 162—179.
[36]	Guibert P, Brodard A, Quiles A, et al. 2015. When were the walls of the Chauvet-Pont d'Arc Cave heated?A chronological approach by thermoluminescence[J]. Quaternary Geochronology, 29: 36—47.
[37]	Guralnik B, Ankjærgaard C, Jain M, et al. 2015a. OSL-thermochronometry using bedrock quartz: A note of caution[J]. Quaternary Geochronology, 25: 37—48.
[38]	Guralnik B, Jain M, Herman F, et al. 2015b. OSL-thermochronometry of feldspar from the KTB borehole, Germany[J]. Earth Planetary Science Letters, 423: 232—243.
[39]	Harmon R S, Thompson P, Schwarcz H P, et al. 1975. Uranium-series dating of speleothems[J]. National Speleological Society Bulletin, 37: 21—33.
[40]	Harmon R S, Thompson P, Schwarcz H P, et al. 1978. Late Pleistocene paleoclimates of North America as inferred from stable isotope studies of Speleothems1[J]. Quaternary Research, 9(1): 54—70.
[41]	Herman F, King G E. 2018. Luminescence thermochronometry: Investigating the link between mountain erosion, tectonics and climate[J]. Elements: An International Magazine of Mineralogy, Geochemistry, Petrology, 14(1): 33—38.
[42]	Herman F, Rhodes E J, Braun J, et al. 2010. Uniform erosion rates and relief amplitude during glacial cycles in the Southern Alps of New Zealand, as revealed from OSL-thermochronology[J]. Earth Planetary Science Letters, 297(1-2): 183—189.
[43]	Hossain S, De Corte F, Vandenberghe D. 2002. A comparison of methods for the annual radiation dose determination in the luminescence dating of loess sediment[J]. Nuclear Instruments Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors Associated Equipment, 490(3): 598—613.
[44]	Hossain S, De Corte F, Vandenberghe D, et al. 2003. The role of k₀-NAA in the assessment of the annual radiation dose for use in TL/OSL dating of sediments[J]. Journal of radioanalytical Radioanalytical nuclear Nuclear chemistryChemistry, 257: 639—642.
[45]	Hu G M, Li S H. 2019. Simplified procedures for optical dating of young sediments using quartz[J]. Quaternary Geochronology, 49: 31—38. DOI
[46]	Huang C, Zhang J J, Wang L B, et al. 2022. Equivalent dose estimation of calcite using isothermal thermoluminescence signals[J]. Quaternary Geochronology, 70: 1—10.
[47]	Huntley D J, Lamothe M. 2001. Ubiquity of anomalous fading in K-feldspars and the measurement and correction for it in optical dating[J]. Canadian Journal of Earth Sciences, 38(7): 1093—1106.
[48]	Jain M, Bøtter-Jensen L, Murray A, et al. 2005. Revisiting TL: Dose measurement beyond the OSL range using SAR[J]. Ancient TL, 23(1): 9—24.
[49]	Jain M. 2000. Stratigraphic development of some exposed Quaternary alluvial sequences in the Thar and its margins: Fluvial response to climate change, Western India[D]. University of Delhi, New Delhi.
[50]	Johnson N M, Blanchard R L. 1967. Radiation dosimetry from the natural thermoluminescence of fossil shells[J]. American Mineralogist: Journal of Earth Planetary Materials, 52(9-10): 1297—1310.
[51]	Johnson N M. 1960. Thermoluminescence in biogenic calcium carbonate[J]. Journal of Sedimentary Research, 30(2): 305—313.
[52]	Johnson N M. 1966. Geothermometry from the thermoluminescence of contact-metamorphosed limestone[J]. The Journal of Geology, 74(5): 607—619.
[53]	Kalita J M, Chithambo M L. 2019. Thermoluminescence and infrared light stimulated luminescence of limestone(CaCO₃)and its dosimetric features[J]. Applied Radiation and Isotopes, 154: 1—7.
[54]	Kang S G, Wang X L, Lu Y C. 2013. Quartz OSL chronology and dust accumulation rate changes since the Last Glacial at Weinan on the southeastern Chinese Loess Plateau[J]. Boreas, 42(4): 815—829.
[55]	Kim K B, Hong D G. 2014. Kinetic parameters, bleaching and radiation response of thermoluminescence glow peaks separated by deconvolution on Korean calcite[J]. Radiation Physics and Chemistry, 13: 16—21.
[56]	King G E, Guralnik B, Valla P G, et al. 2016a. Trapped-charge thermochronometry and thermometry: A status review[J]. Chemical Geology, 446: 3—17.
[57]	King G E, Herman F, Guralnik B. 2016b. Northward migration of the eastern Himalayan syntaxis revealed by OSL thermochronometry[J]. Science, 353(6301): 800—804.
[58]	Kirsh Y, Townsend P D, Shoval S. 1987. Local transitions and charge transport in thermoluminescence of calcite[J]. International Journal of Radiation Applications Instrumentation(Part D), Nuclear Tracks Radiation Measurements, 13(2-3): 115—119.
[59]	Kong P, Granger D E, Wu F Y, et al. 2009. Cosmogenic nuclide burial ages and provenance of the Xigeda paleo-lake: Implications for evolution of the Middle Yangtze River[J]. Earth Planetary Science Letters, 278(1-2): 131—141.
[60]	Koul D K, Bhat C L. 1995. TLPLAT: A program for the identification of plateau in thermoluminescence studies[J]. Computers Geosciences, 21(3): 409—412.
[61]	Koul D K. 1994. Plateau identification in thermoluminescence studies[J]. Applied Radiation Isotopes, 45(12): 1201—1206.
[62]	Lacassin R, Schärer U, Leloup P H, et al. 1996. Tertiary deformation and metamorphism SE of Tibet: The folded Tiger-leap décollement of NW Yunnan, China[J]. Tectonics, 15(3): 605—622.
[63]	Lai Z, Brückner H, Fülling A, et al. 2008. Effects of thermal treatment on the growth curve shape for OSL of quartz extracted from Chinese loess[J]. Radiation Measurements, 43(2-6): 763—766.
[64]	Li B, Jacobs Z, Roberts R G. 2017. An improved multiple-aliquot regenerative-dose(MAR)procedure for post-IR IRSL dating of K-feldspar[J]. Ancient TL, 35(1): 1—10.
[65]	Li B, Li S H. 2011. Luminescence dating of K-feldspar from sediments: a protocol without anomalous fading correction[J]. Quaternary Geochronology, 6(5): 468—479.
[66]	Li B, Li S H. 2012. Determining the cooling age using luminescence-thermochronology[J]. Tectonophysics, 580: 242—248.
[67]	Li S H, Chen Y Y, Li B, et al. 2007. OSL dating of sediments from deserts in northern China[J]. Quaternary Geochronology, 2(1-4): 23—28.
[68]	Liritzis I, Guibert P, Foti F, et al. 1996. Solar bleaching of thermoluminescence of calcites[J]. Nuclear Instruments Methods in Physics Research Section B: Beam Interactions with Materials Atoms, 117(3): 260—268.
[69]	Liritzis I. 1994. A new dating method by thermoluminescence of carved megalithic stone builing[J]. Académie des sciences, 319: 603—610.
[70]	Liritzis I. 2010. Strofilas(Andros Island, Greece): New evidence for the cycladic final neolithic period through novel dating methods using luminescence and obsidian hydration[J]. Journal of Archaeological Science, 37(6): 1367—1377.
[71]	Liu-Zeng J, Tapponnier P, Gaudemer Y, et al. 2008. Quantifying landscape differences across the Tibetan plateau: Implications for topographic relief evolution[J]. Journal of Geophysical Research: Earth Surface, 113(F4): 1—26.
[72]	Lowick S E, Preusser F, Pini R, et al. 2010. Underestimation of fine grain quartz OSL dating towards the Eemian: comparison with palynostratigraphy from Azzano Decimo, northeastern Italy[J]. Quaternary Geochronology, 5(5): 583—590.
[73]	Lu Y C, Wang X L, Wintle A G. 2007. A new OSL chronology for dust accumulation in the last 130 000yr for the Chinese Loess Plateau[J]. Quaternary Research, 67(1): 152—160.
[74]	Madsen A T, Murray A S. 2009. Optically stimulated luminescence dating of young sediments: A review[J]. Geomorphology, 109(1-2): 3—16.
[75]	Matsuoka M, Takatohi U E, Watanabe S, et al. 1983. TL dating of fish fossil from Brazil[J]. Radiation Protection Dosimetry, 6(1-4): 185—188.
[76]	Mckeever S W. 1985. Thermoluminescence of Solids[M]. Cambridge University Press, Cambridge.
[77]	Misdaq M A, Oufni L, Erramli H, et al. 2002. Dating of a quaternary limestone cave by combining the SSNTD technique with paleodose measurements: Application to the stalagmite and stalactite growth[J]. Radiation Measurements, 35(4): 339—345.
[78]	Morthekai P, Jain M, Murray A, et al. 2008. Fading characteristics of martian analogue materials and the applicability of a correction procedure[J]. Radiation Measurements, 43(2-6): 672—678.
[79]	Moska P, Murray A S. 2006. Stability of the quartz fast-component in insensitive samples[J]. Radiation Measurements, 41(7-8): 878—885.
[80]	Murray A, Wintle A G. 2000a. Application of the single-aliquot regenerative-dose protocol to the 375℃ quartz TL signal[J]. Radiation Measurements, 32(5-6): 579—583.
[81]	Murray A, Wintle A G. 2000b. Luminescence dating of quartz using an improved single-aliquot regenerative-dose protocol[J]. Radiation Measurements, 32(1): 57—73.
[82]	Ninagawa K, Adachi K, Uchimura N, et al. 1992. Thermoluminescence dating of calcite shells in the pectinidae family[J]. Quaternary Science Reviews, 11(1): 121—126.
[83]	Ninagawa K, Kitahara T, Toyoda S, et al. 2001. Thermoluminescence dating of the Ryukyu Limestone[J]. Quaternary Science Reviews, 20(5): 829—833.
[84]	Ninagawa K, Matsukuma Y, Fukuda T, et al. 1994. Thermoluminescence dating of a calcite shell, crassostrea gigas(Thunberg)in the ostreidae family[J]. Quaternary Science Reviews, 13(5-7): 589—593.
[85]	Ogata M, Hasebe N, Fujii N, et al. 2017. Measuring apparent dose rate factors using beta and gamma rays, and alpha efficiency for precise thermoluminescence dating of calcite[J]. Journal of Mineralogical Petrological Sciences, 112(6): 336—345.
[86]	Pagonis V, Baker A, Larsen M, et al. 2011. Precision and accuracy of two luminescence dating techniques for retrospective dosimetry: SAR-OSL and SAR-ITL[J]. Nuclear Instruments Methods in Physics Research Section B: Beam Interactions with MaterialsAtoms, 269(7): 653—663.
[87]	Polikreti K, Michael C T, Maniatis Y. 2003. Thermoluminescence characteristics of marble and dating of freshly excavated marble objects[J]. Radiation Measurements, 37(1): 87—94.
[88]	Prescott J R, Hutton J T. 1994. Cosmic ray contributions to dose rates for luminescence and ESR dating: Large depths and long-term time variations[J]. Radiation Measurements, 23(2-3): 497—500.
[89]	Qin J T, Zhou L P. 2012. Effects of thermally transferred signals in the post-IR IRSL SAR protocol[J]. Radiation Measurements, 47(9): 710—715.
[90]	Qin J T, Zhou L P. 2018. Luminescence dating of the Zeketai loess section in the Ili Basin, Northwestern China: Methodological considerations[J]. Journal of Asian Earth Sciences, 155: 146—153.
[91]	Rahimzadeh N, Tsukamoto U, Zhang J J, et al. 2021. Natural and laboratory dose response curves of quartz violet stimulated luminescence(VSL): Exploring the multiple aliquot regenerative dose(MAR)protocol[J]. Quaternary Geochronology, 65(1): 1—8.
[92]	Roberts H M. 2008. The development and application of luminescence dating to loess deposits: A perspective on the past, present and future[J]. Boreas, 37(4): 483—507.
[93]	Roberts R G, Spooner N A, Questiaux D G. 1994. Palaeodose underestimates caused by extended-duration preheats in the optical dating of quartz[J]. Radiation Measurements, 23(2-3): 647—653.
[94]	Roque C, Guibert P, Vartanian E, et al. 2001. Thermoluminescence—dating of calcite: Study of heated limestone fragments from Upper Paleolithic layers at Combe Sauniere, Dordogne, France[J]. Quaternary Science Reviews, 20(5-9): 935—938.
[95]	Rosenberg T M, Preusser F, Wintle A G. 2011. A comparison of single and multiple aliquot TT-OSL data sets for sand-sized quartz from the Arabian Peninsula[J]. Radiation Measurements, 46(6-7): 573—579.
[96]	Rui X, Li B, Guo Y J. 2020. Testing the upper limit of luminescence dating based on standardised growth curves for MET-pIRIR signals of K-feldspar grains from northern China[J]. Quaternary Geochronology, 57:101063.
[97]	Shen X, Tian Y, Li D, et al. 2016. Oligocene-Early Miocene river incision near the first bend of the Yangze River: Insights from apatite (U-Th-Sm)/He thermochronology[J]. Tectonophysics, 687: 223—231.
[98]	Sohbati R, Murray A S, Jain M, et al. 2011. Investigating the resetting of OSL signals in rock surfaces[J]. Geochronometria, 38(3): 249—258.
[99]	Soliman C, Metwally S M. 2006. Thermoluminescence of the green emission band of calcite[J]. Radiation Effects and Defects in Solids, 161(10): 607—613.
[100]	Spooner N A. 1992. Optical dating: Preliminary results on the anomalous fading of luminescence from feldspars[J]. Quaternary Science Reviews, 11(1): 139—145.
[101]	Spooner N A. 1993. The Validity of Optical Dating Based on Feldspar[D]. University of Oxford, Oxford.
[102]	Spooner N A. 1994. The anomalous fading of infrared-stimulated luminescence from feldspars[J]. Radiation Measurements, 23(2-3): 625—632.
[103]	Sutton S R, Zimmerman D W. 1976. Thermoluminescent dating using zircon grains from archaeological ceramics[J]. Archaeometry, 18: 125—134.
[104]	Tang S L, Li S H. 2015. Low temperature thermochronology using thermoluminescence signals from quartz[J]. Radiation Measurements, 81: 92—97.
[105]	Thomsen K J, Murray A S, Jain M, et al. 2008. Laboratory fading rates of various luminescence signals from feldspar-rich sediment extracts[J]. Radiation Measurements, 43(9-10): 1474—1486.
[106]	Timar A, Vandenberghe D, Panaiotu E C, et al. 2010. Optical dating of Romanian loess using fine-grained quartz[J]. Quaternary Geochronology, 5(2-3): 143—148.
[107]	Vandergoes M J, Newnham R M, Preusser F, et al. 2005. Regional insolation forcing of late Quaternary climate change in the Southern Hemisphere[J]. Nature, 436(7048): 242—245.
[108]	Visocekas R. 1979. Miscellaneous aspects of artificial TL of calcite: Emission spectra, athermal detrapping and anomalous fading[J]. Physics and Chemistry of the Earth, 3: 258—265.
[109]	Visocekas R. 1985. Tunnelling radiative recombination in labradorite: Its association with anomalous fading of thermoluminescence[J]. Nuclear Tracks and Radiation Measurements(1982), 10(4): 521—529.
[110]	Visocekas R. 2002. Tunnelling in Afterglow: Its coexistence and interweaving with thermally stimulated luminescence[J]. Radiation Protection Dosimetry, 100(1-4): 45—53.
[111]	Wang X, Lu Y, Zhao H. 2006. On the performances of the single-aliquot regenerative-dose(SAR)protocol for Chinese loess: fine quartz and polymineral grains[J]. Radiation Measurements, 41(1): 1—8.
[112]	Wary J L. 1957. Precipitation of calcite and aragonite[J]. Journal of the American Chemical Society, 79(9): 2031—2034.
[113]	Whipple K X, Tucker G E. 1999. Dynamics of the stream-power river incision model: Implications for height limits of mountain ranges, landscape response timescales, and research needs[J]. Journal of Geophysical Research: Solid Earth, 104(B8): 17661—17674.
[114]	Willett S D, McCoy S W, Perron J T, et al. 2014. Dynamic reorganization of river basins[J]. Science, 343(1248765): 1—9.
[115]	Wintle A G, Adamiec G. 2017. Optically stimulated luminescence signals from quartz: A review[J]. Radiation Measurements, 98: 10—33.
[116]	Wintle A G, Dijkmans J. 1988. Dose-rate comparisons of sands for thermoluminescence dating[J]. Acient TL, 6(6): 15—17.
[117]	Wintle A G. 1973. Anomalous fading of thermo-luminescence in mineral samples[J]. Nature, 245(5421): 143—144.
[118]	Wintle A G. 1974. Factors Determining the Thermoluminescence of Chronologically Significant Materials[D]. University of Oxford, Oxford.
[119]	Wintle A G. 1978. A thermoluminescence dating study of some Quaternary calcite: Potential and problems[J]. Canadian Journal of Earth Sciences, 15(12): 1977—1986.
[120]	Wintle A G. 1997. Luminescence dating: Laboratory procedures and protocols[J]. Radiation Measurements, 27(5-6): 769—817.
[121]	Wissink G K, Hoke G D, Garzione C N, et al. 2016. Temporal and spatial patterns of sediment routing across the southeast margin of the Tibetan plateau: Insights from detrital zircon[J]. Tectonics, 35(11-12): 2538—2563.
[122]	Wu T S, Jain M, Guralnik B, et al. 2015. Luminescence characteristics of quartz from Hsuehshan Range(Central Taiwan)and implications for thermochronometry[J]. Radiation Measurements, 81: 104—109.
[123]	Yan Y, Carter A, Huang C Y, et al. 2012. Constraints on Cenozoic regional drainage evolution of SW China from the provenance of the Jianchuan Basin[J]. Geochemistry Geophysics Geosystems, 13(3): 1—12.
[124]	Yee K P, Mo R H. 2018. Thermoluminescence dating of stalactitic calcite from the early Palaeolithic occupation at Tongamdong site[J]. Journal of Archaeological Science: Reports, 19: 405—410.
[125]	Zhang J J, Wang L B. 2020. Thermoluminescence dating of calcite: Alpha effectiveness and measurement protocols[J]. Journal of Luminescence, 223(117205): 1—8.
[126]	Zheng H B, Clift P D, Wang P, et al. 2013. Pre-miocene birth of the Yangtze River[J]. Proceedings of the National Academy of Sciences, 110(19): 7556—7561.
[127]	Zhou L P, Shackleton N J. 2001. Photon-stimulated luminescence of quartz from loess and effects of sensitivity change on palaeodose determination[J]. Quaternary Science Reviews, 20(5-9): 853—857.

方解石热释光定年技术的发展历史与展望

DEVELOPMENT AND PROSPECT OF THERMOLUMINESCENCE DATING BY USING CALCITE

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